Powder injection moulding based on a novel binder system, and using 31
6L stainless steel powder as a test material, is described. The binder
system comprises a major fraction of polyethyleneglycols (PEGs) of va
rious molecular weights and a minor fraction of very finely dispersed
polymethylmethacrylate (PMMA) incorporated in the form of an emulsion.
The feedstock was mixed as a thick, aqueous slurry at room temperatur
e and was rapidly homogenised by stirring at a low shear force, which
should minimise contamination because of a much reduced wear rate of t
he mixing equipment. The possible demixing during the drying of the sl
urry was minimised by frequent stirring during this stage and the use
of some shear mixing of the dried feedstock. The green strength of the
moulded specimens was measured by a three point bend test. In the fir
st stage of debinding, the PEGs were removed by water leaching from th
e moulded components. This opened up pore channels which allowed much
faster removal of the remaining PMMA binder during subsequent thermal
debinding. The debinded samples were sintered at different temperature
s and the sintered samples were examined by SEM and optical microscopy
for pore structure and defects such as cracks.