Y. Leduigou et al., A CONTROLLED POTENTIAL COULOMETER FOR HIGH-PRECISION URANIUM AND PLUTONIUM ANALYSIS .1. DESCRIPTION AND ELECTRICAL TEST, Fresenius' journal of analytical chemistry, 351(6), 1995, pp. 493-498
A controlled potential coulometer has been constructed according to sp
ecific requirements which are relevant for high precision analytical w
ork. The working of the instrument electronics is described together w
ith its electrical calibration. Emphasis has been put on the delivery
and measurement of a low current at the end of the electrolysis. A rel
iable scheme for an accurate calibration of the coulometer has been wo
rked out.