Mc. Freitas, ELEMENTAL CONCENTRATIONS IN THE SPINACH REFERENCE MATERIAL DETERMINEDBY K(O)-BASED INAA, Fresenius' journal of analytical chemistry, 352(1-2), 1995, pp. 58-60
The IAEA-331 spinach material NIST SRM 1570a Spinach Leaves, submitted
to an intercomparison run by the IAEA, has been analysed by k(0)-base
d INAA with counting using both low and high energy photon detectors.
The results have been compared with (i) the certified values of the NI
ST SRM 1570a; the agreement is good, taking into account the uncertain
ties; and (ii) the certified and ''consensus'' values of the former NI
ST SRM 1570 Spinach Leaves, their composition in minor and trace-eleme
nts are quite similar; however a lower content has been observed for C
o, Fe and Sc in the IAEA-331 and for Zn in the SRM 1570. For quality c
ontrol, the NIST 1573 Tomato Leaves and the NIST 1575 Pine Needles hav
e been analysed using the same conditions as for the IAEA-331. The res
ults agree quite well with the certified and ''consensus'' values give
n in the literature.