Tf. Walsh et Ce. Bakis, THE EFFECT OF HIGH-TEMPERATURE DEGRADATION ON THE MODE-I CRITICAL STRAIN-ENERGY RELEASE RATE OF A GRAPHITE EPOXY COMPOSITE/, Journal of composites technology & research, 17(3), 1995, pp. 228-234
The double cantilever beam (DCB) test was used to determine the effect
s of high-temperature degradation on the Mode I critical strain energy
release rate (G(IC)) of a continuous fiber-reinforced polymer-matrix
composite material. The composite material investigated was IM7/8551-7
A graphite/rubber-toughened epoxy system. Delamination starter films o
f two different thicknesses were used: 25.4 mu m and 12.7 mu m. High-t
emperature degradation was accomplished by placing the specimens on a
wire rack in a forced-air convection oven held at 177 degrees C. A con
tinuous flow of fresh laboratory air existed at all times. G(IC) decre
ased with increased exposure, showing a 40% reduction after 8000 h. Th
e specimens with thicker inserts showed a higher G(IC). Weight loss of
the material occurred throughout the aging cycle, indicating that the
rmo-oxidation was occurring. G(IC) was not affected by the wedging ope
n of the precrack during exposure. Crack propagation in the unexposed
specimens occurred in the matrix material, whereas for the exposed spe
cimens, it occurred along the fiber-matrix interface. This indicated p
ossible exposure-induced interfacial degradation.