EFFECT OF STARCH PASTE CONCENTRATION ON PARTICLE-SIZE DISTRIBUTION OFFINE GRANULES PRODUCED BY AGITATION GRANULATION

Particle size distribution of fine granules produced by agitation gran ulation was investigated as a function of the concentration of starch paste, The time course of granulation was investigated in a high speed type mixer using 5% starch paste having a good fluidity and 15% starc h paste having no fluidity at all, like a gel, In agitation granulatio n, aggregation and deaggregation of particles and/or granules occurred simultaneously. At a low concentration of starch paste, massing of th e granules, namely the growth of granules, occurred mainly during the agitation granulation, since the relatively large amount of free water was available from the paste, Therefore, in this case, only the mean size shifted toward a larger measurement without any change in the wid th of the granules during the granulation. At a high concentration of starch paste, rapid deaggregation of granules by shear force applied o ccurred following the formation of large granules immediately after th e addition of paste, Since a small amount of water exudes from the pas te during the agitation, massing proceeds slowly, This means that in t he case of granulation using a high concentration of starch paste, dea ggregation proceeds predominantly, so that the size distribution of th e granules becomes more narrow, Fine granules may be produced by agita tion granulation when a high concentration of starch paste is used and when granulation is executed under sufficient shear or rotation speed that guarantees satisfactory dispersion of the gel.