S. Stassen et al., MAGNETIC ALIGNMENT IN 2212-BI-BASED SUPERCONDUCTING SYSTEM .2. BI2SR2CA1-XDYXCU2O8-Y X=0.2 GLASS RECRYSTALLIZED IN 0.6 T MAGNETIC-FIELD, Journal of materials research, 10(8), 1995, pp. 1878-1883
Starting from a glassy precursor, Bi2Sr2Ca1-xDyxCu2O8-y (for x = 0.2)
was recrystallized under a 0.6 T magnetic field. After splat quenching
, the samples were heated and sintered at different temperatures T-1,
then slowly cooled. X-ray diffraction data, sometimes showing 00l peak
splitting and electron scanning microscopy pictures, were collected.
The results showed that the magnetic field could orient the grains and
led to a magnetically textured growth process. Secondary phases forme
d in the system during this process were identified by EDX analysis. T
he optimum T-1 for texturing was found to be between 930 degrees C and
950 degrees C.