We describe a method of uranium-thorium-lead (U-Th-Pb) isotopic age da
ting for Quaternary rocks. The approach uses an instrumental mass disc
rimination correction for lead isotope ratios, which allows small enri
chments of radiogenic Pb-206 and Pb-208 to be detected at the level of
0.001%. Igneous rocks hosting minerals with a range in U-238/Pb-204 v
alues of 100 can be dated with uncertainties of approximately +/- 15-2
0 kyr. A Quatemary rhyolite dated at 1.19 Ma by K-Ar yields a U-238-Pb
-206 age of 1.03 +/- 0.10 Ma. A Holocene dacite (9.5 ka) has uniform P
b-206/Pb-207 to within +/- 0.0015% in groundmass phases, but 1 mm plag
ioclase phenocrysts have lower Pb-206/Pb-207 by 0.105 +/- 0.002% indic
ating contamination of the magma after plagioclase crystallization. Hi
gh precision Pb-206/Pb-207 ratios may be a useful new tool for petroge
netic studies.