PREPARATION OF NICKEL-COATED ALUMINA COMPOSITE POWDER BY AN AQUEOUS-PHASE REDUCTION PROCESS

Citation
Bs. Kang et al., PREPARATION OF NICKEL-COATED ALUMINA COMPOSITE POWDER BY AN AQUEOUS-PHASE REDUCTION PROCESS, Journal of Materials Science, 30(15), 1995, pp. 3883-3887
Citations number
12
Categorie Soggetti
Material Science
ISSN journal
00222461
Volume
30
Issue
15
Year of publication
1995
Pages
3883 - 3887
Database
ISI
SICI code
0022-2461(1995)30:15<3883:PONACP>2.0.ZU;2-1
Abstract
A nickel coating on the surface of alumina particles, used as a reinfo rcement in metal-ceramic composite materials, substantially improves t heir wettability by molten metals. Nickel was deposited on alumina par ticles by reducing nickel ions from a solution under hydrogen pressure in the presence of ammonia as a complexing agent. It was found that t he addition of Fe2+ ions and anthraquinone was necessary for forming a n adequate nickel coating on the alumina surface. The optimum conditio ns were the [NH3]/[Ni2+] ratio of 1.6, 2760 kPa hydrogen pressure, 175 degrees C, and an anthraquinone addition of 0.04 gl(-1).