Kv. Salazar et al., EFFECTS OF OXYGEN PARTIAL-PRESSURE AND MECHANICAL DEFORMATION ON (TL,PB) (BA,SR)(2)CA2CU3OY AG-SHEATHED TAPES, IEEE transactions on applied superconductivity, 5(2), 1995, pp. 1494-1497
The powder in tube method was used to produce silver sheathed tapes of
Tl0.78Pb0.5Ba0.4Sr1.6Ca2Cu3Oy. A precursor powder of Pb0.5Ba0.4Sr1.6C
a2Ca3Oy (prepared via the hydroxycarbonate coprecipitation of the meta
l ions from a stoichiometric nitrate solution) was thallinated and pac
ked into a silver tube and processed into tape. The tape was then heat
ed (in 100% oxygen or air) from 840 degrees C to 870 degrees C for var
ious anneal times. The effects of different intermediate pressing stre
sses during tape processing had dramatic effects on both the current-c
arrying capacity and the tape microstructure. Variation of pO(2) also
led to differences in current-carrying capacity I-c as did a roll subs
tituted for a press during tape processing.