Mb. Field et al., EXPERIMENTAL-EVIDENCE FOR ELECTROMAGNETIC COUPLING INHOMOGENEITY ALONG THE GRAIN-BOUNDARY PLANE IN HIGH-ANGLE MELT-TEXTURED YBA2CU3O6+X, IEEE transactions on applied superconductivity, 5(2), 1995, pp. 1631-1634
Detailed characterization of two high angle general misorientation YBa
2Cu3O6+x bicrystals produced by the melt-texture-liquid-phase-removal
method shows that the boundaries contain regions of both strong and we
ak coupling, In one bicrystal the strongly coupled component was infer
red from analysis of the magnetic-field-dependent voltage-current char
acteristics and confirmed with magneto-optical images of the boundary.
Several sections of the second sample having macroscopically differen
t grain boundary facets were tested after sectioning with a laser. The
properties were not dependent on the grain boundary plane orientation
. High-field, high-sensitivity voltage-current characteristics of the
inter and intra-grain regions had qualitatively identical properties a
nd confirmed that there was a substantial strong coupled component to
the boundary. The data confirm that the melt-texture-liquid-phase-remo
val method of YBa2Cu3O6+x formation is beneficial to the formation of
strong-coupling regions in high angle grain boundaries and that some h
igh angle grain boundaries contain strongly coupled components.