Be. Wilde et al., THE INFLUENCE OF LASER-SURFACE MELTING ON THE RESISTANCE OF AISI-4135LOW-ALLOY STEEL TO HYDROGEN-INDUCED BRITTLE-FRACTURE, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 198(1-2), 1995, pp. 43-49
Flat and cylindrical heat-treated AISI 4135 low alloy steel specimens
were surface treated using power levels of 50, 100 and 200 W. The resu
lts of hydrogen permeation and slow strain rate tension (SSRT) tests s
how the following. (1) Laser surface treatment of AISI 4135 low alloy
steel results in a reduction in the hydrogen absorption kinetics as me
asured by the permeation test: and also an improved resistance to hydr
ogen-induced fracture in the SSRT test under galvanostatic charging co
nditions. (2) The degree of effectiveness in reducing the hydrogen abs
orption rate is shown to occur at all power levels, and is greatest at
the 50 W level. (3) A clear qualitative relationship is described bet
ween the hydrogen absorption rate and the time to failure in the SSRT
test. This relation was even more striking in terms of the fractograph
ic detail of the fracture face. (4) A possible explanation for the red
uced hydrogen absorption as a result of low power laser surface meltin
g treatment is the influence of the rapidly quenched metal surface on
the steady state degree of hydrogen adatom coverage or the absorption
kinetic rate constant or both. (5) Reverse membrane permeation experim
ents indicated that the effect of laser surface melting on the permeat
ion flux at constant charging current was not due to barriers in the m
etal which alter the hydrogen flux gradient across the membrane.