[(YBaCuO)(m)/(PrBaCuO)(n)](10) multilayers have been deposited by Meta
l Organic Chemical Vapor Deposition (MOCVD). The films grow on SrTiO3
(100) and MgO (100) substrates and have c-axis perpendicular to the su
bstrate. A serie of superlattices has been synthesised with different
deposition temperatures ranging between 700 and 850 degrees C with dif
ferent modulations (the thickness of YBCO layers staying unchanged and
equal to 100 Angstrom). The elements concentrations profiles at the i
nterfaces and the interdiffusion were determined by secondary neutral
mass spectroscopy (SNMS). X-ray diffraction show satellite peaks (char
acteristic of superlattice modulation) around 001 and 002 reflections.
Moreover, the samples show a good in-plane orientation. The supercond
ucting properties are analysed by AC screening. The critical temperatu
re reaches 88K in the case of m=8 and n=2 (n and m being the numbers o
f units cells along c-axis for YBCO layer and PBCO one respectively).