P. Quevauviller et al., CERTIFIED REFERENCE MATERIALS OF SOILS AND SEWAGE SLUDGES FOR THE QUALITY-CONTROL OF TRACE-ELEMENT ENVIRONMENTAL MONITORING, TrAC. Trends in analytical chemistry, 15(10), 1996, pp. 504-513
For the wide variety of soil/sludge matrices encountered in analytical
practice, a range of CRMs should be available to verify the analytica
l quality control of any determination carried out, using samples whic
h should be as similar as possible to real soil and sludge samples so
that the method's performance may be tested under real analytical cond
itions. This paper presents basic requirements for the preparation of
soil and sludge CRMs for the quality control of trace element determin
ations (total and extractable contents, following strict extraction pr
otocols), and gives recent examples of new certifications successfully
concluded by the SM&T programme of the European Commission.