ON-SITE SOLID-PHASE EXTRACTION AND COUPLED-COLUMN HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF 6 POLYCYCLIC AROMATIC-HYDROCARBONS IN WATER

Authors
LINTELMANN J WAADT K SAUERBREY R KETTRUP A
Citation
J. Lintelmann et al., ON-SITE SOLID-PHASE EXTRACTION AND COUPLED-COLUMN HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF 6 POLYCYCLIC AROMATIC-HYDROCARBONS IN WATER, Fresenius' journal of analytical chemistry, 352(7-8), 1995, pp. 735-742
Citations number
36
Categorie Soggetti
Chemistry Analytical
Journal title
Fresenius' journal of analytical chemistry → ACNP
ISSN journal
09370633
Volume
352
Issue
7-8
Year of publication
1995
Pages
735 - 742
Database
ISI
SICI code
0937-0633(1995)352:7-8<735:OSEACH>2.0.ZU;2-X
Abstract
A high-performance liquid chromatographic method for the determination of fluoranthene, benzo(b)fluoranthene, benzo (k)fluoranthene, benzo(a )pyrene, benzo(g,h,i)perylene and indeno(1,2,3-cd)pyrene in water is p resented. The analytical procedure consists of on-site solid-phase ext raction of the analytes on a selective sample column using a new devic e, transport and integration of the loaded sample column into a HPLC-s ystem and coupled-column HPLC-analysis. The method allows reliable qua ntification of the PAHs at the low ng/l-level in particle-free as well as in particle-containing surface water.