T. Buyukyilmaz et al., THE EFFECT ON THE TENSILE BOND STRENGTH OF ORTHODONTIC BRACKETS OF TITANIUM TETRAFLUORIDE (TIF4) APPLICATION AFTER ACID ETCHING, American journal of orthodontics and dentofacial orthopedics, 108(3), 1995, pp. 256-261
Titanium tetrafluoride (TiF4) was applied to acid-etched enamel surfac
es to study the effect on surface structure and tensile bond strength
of orthodontic brackets. Three groups of 20 premolars each were compar
ed in debonding tests. Group I received a 1% and Group II received a 4
% topical TIF4 treatment after acid etching. Group III served as contr
ol, that is, no fluoride solution was applied to the enamel after acid
etching. Each treatment lasted 60 seconds followed by a thorough rins
ing with water for 30 seconds. Brackets were bonded on all teech with
the same procedure. All premolars were then placed in a water bath at
37 degrees C. Ten teeth from each group were debonded after 24 hours,
and the remaining teeth were debonded after 6 months. Results indicate
d that the application of 1% and 4% TIF4 solutions on etched enamel su
rfaces did not alter the tensile bond strength significantly after 24
hours and 6 months. The scanning electron microscope (SEM) examination
of the surface structure demonstrated the presence of extensive react
ion products, which covered enamel surfaces and appeared to interfere
with etch patterns. It was concluded that the application of TIF4 solu
tions to etched enamel surfaces before bonding will not have an advers
e effect on the tensile strength of orthodontic attachments.