A SECURE AND CONVENIENT SYNTHESIS OF 5-AMINO-1,2,3-THIADIAZOLE BY DIAZOACETONITRILE

Authors
HARADA K MORI Y NAKAI M
Citation
K. Harada et al., A SECURE AND CONVENIENT SYNTHESIS OF 5-AMINO-1,2,3-THIADIAZOLE BY DIAZOACETONITRILE, Heterocycles, 44, 1997, pp. 197-201
Citations number
15
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Heterocycles → ACNP
ISSN journal
03855414
Volume
44
Year of publication
1997
Pages
197 - 201
Database
ISI
SICI code
0385-5414(1997)44:<197:ASACSO>2.0.ZU;2-#
Abstract
A new synthesis of 5-amino-1,2,3-thiadiazole (3) by diazoacetonitrile (2) and H2S in the presence of a base is described The compound (2) is undoubtedly explosive but with our method we found it could be used f or industrial purposes.