Xa. Wu et Kh. Bellgardt, ONLINE FAULT-DETECTION OF FLOW-INJECTION ANALYSIS SYSTEMS BASED ON RECURSIVE PARAMETER-ESTIMATION, Analytica chimica acta, 313(3), 1995, pp. 161-176
Effective automated supervision can help to ensure the reliable operat
ion of complex flow-injection analysis (FIA) systems. As an important
element of a supervisory system, fast fault detection of the FIA syste
ms is required. In this paper, a model-based fault detection method ba
sed on the identification of the model parameters is developed. The fa
ult detection system consists of the three levels estimation, filterin
g and evaluation of the model parameters. The model order and the time
delay of the system are determined on-line. The recursive fixed memor
y (RFM) method is used to estimate model parameters. The fault detecti
on of a FIA system is performed by means of filtering the estimated mo
del parameters through a high- and low-pass filter for separation of f
aults with different magnitude in their dynamics. The application to d
ifferent practical examples confirms that the newly developed method o
ffers a very effective way for fault detection in the FIA process.