ATOMIC-FORCE MICROSCOPY INVESTIGATION OF TENSILE-STRESSED SILICON GROWN BY RAPID THERMAL CHEMICAL-VAPOR-DEPOSITION ON SI0.68GE0.32 RELAXED PSEUDO-SUBSTRATES
F. Chollet et al., ATOMIC-FORCE MICROSCOPY INVESTIGATION OF TENSILE-STRESSED SILICON GROWN BY RAPID THERMAL CHEMICAL-VAPOR-DEPOSITION ON SI0.68GE0.32 RELAXED PSEUDO-SUBSTRATES, JPN J A P 1, 33(12A), 1994, pp. 6437-6442
Rapid thermal chemical vapour deposition (RTCVD) has been applied to t
he growth of silicon layers under tensile stress on relaxed Si0.68Ge0.
32 buffer layers at 610 and 810 degrees C. Their surface morphology wa
s characterised with atomic height resolution by Tapping-mode atomic f
orce microscopy (TM-AFM). While a uniform isotropic nanoroughness is r
evealed on pseudo-substrates, a quite different roughness can be obser
ved for silicon films. For high temperature grown films, high surface
diffusion rates of adsorbed species enable an extended reconstruction
of the Si (100) surface: large domains showing terraces as well as fac
eted planes appear; the resulting non-uniform silicon film exhibits ea
rly mechanical failure. In contrast, low temperature grown Si films ex
hibit almost the same morphology as pseudo-substrates for thicknesses
up to 15 nm with no apparent mechanical failure. For thicknesses beyon
d 20 nm, terraces form on the steepest part of the slopes, whereas bey
ond 80 nm [110] slip lines indicate the plastic yield of the film.