CRYSTAL AND MOLECULAR-STRUCTURE OF 7A,8A-TETRAAZACYCLOPENTA[DEF]FLUORENE-4,8-DITHIONE

Authors
GIELING GTW NOLTE RJM SCHEEREN JW SMITS JMM BEURSKENS PT BEURSKENS G
Citation
Gtw. Gieling et al., CRYSTAL AND MOLECULAR-STRUCTURE OF 7A,8A-TETRAAZACYCLOPENTA[DEF]FLUORENE-4,8-DITHIONE, Journal of chemical crystallography, 25(7), 1995, pp. 421-424
Citations number
8
Categorie Soggetti
Crystallography,Spectroscopy
Journal title
Journal of chemical crystallography → ACNP
ISSN journal
10741542
Volume
25
Issue
7
Year of publication
1995
Pages
421 - 424
Database
ISI
SICI code
1074-1542(1995)25:7<421:CAMO7>2.0.ZU;2-A
Abstract
The title compound C20H18N4O2S2 crystallizes in the monoclinic space g roup P2(1)/n with a = 8.4930(1) Angstrom, b = 11.4880(1) Angstrom, c = 20.0709(2) Angstrom, beta = 94.933(1)degrees, V = 1951.01(3) Angstrom (3), Z = 4. The crystal structure has been solved by vector search met hods and refined by full-matrix least-squares to R = 0.04 for 2888 ref lections and 116 restraints. The title compound has a suitable geometr y for synthesizing receptor molecules with a cleft for selective compl exation.