REVERSE-PHASE LIQUID-CHROMATOGRAPHY OF P-TERT-BUTYLCALIXARENES

Authors
VOCANSON F LAMARTINE R DUCHAMP C DEVAINS JBR
Citation
F. Vocanson et al., REVERSE-PHASE LIQUID-CHROMATOGRAPHY OF P-TERT-BUTYLCALIXARENES, Chromatographia, 41(3-4), 1995, pp. 204-206
Citations number
12
Categorie Soggetti
Chemistry Analytical","Biochemical Research Methods
Journal title
Chromatographia → ACNP
ISSN journal
00095893
Volume
41
Issue
3-4
Year of publication
1995
Pages
204 - 206
Database
ISI
SICI code
0009-5893(1995)41:3-4<204:RLOP>2.0.ZU;2-H
Abstract
The p-tert-butylcalix[n] arenes (n = 4,6,7,8) and p-tert-butyldihomoox acalix[4]arene have been separated by reverse phase liquid chromatogra phy. Optimum conditions have been obtained on a Spherisorb ODS1, 5 mu m C18 column by isocratic ambient elution with acetonitrile-methyl ter t-butyl ether. Calibration plots have been obtained from purified cali xarenes and the reliability of the method is confirmed from test mixtu res of calixarenes of known composition.