Jm. Calderonmoreno et al., MICROSTRUCTURE AND CREEP-PROPERTIES OF ALUMINA ZIRCONIA CERAMICS/, Journal of the European Ceramic Society, 15(10), 1995, pp. 983-988
High temperature creep of two zirconia roughened alumina ceramics, fab
ricated by powder processing and sol-gel precursors processing, has be
en studied in order to determine plastic determine mechanisms. Compres
sive creep tests were carried out between 1300 and 1450 degrees C, tin
der stresses from 10 to 150 MPa. For the sample fabricated from powder
s, a stress exponent of 1.4 and an activation energy of 580 kJ/mol wer
e found below a critical stress of 40 MPa. For larger stresses, accele
rated creep rates developed. In the specimens processed from precursor
s, values of 1.8 for the stress exponent and 540 kJ/mol for the activa
tion energy, over the entire range of stresses have been determined Cr
eep parameters and microstructural evolution of the samples during the
experiments have been correlated with models to establish the dominan
t creep mechanism.