Y. Takezawa et al., NOVEL DIAGNOSIS OF THERMAL DETERIORATION FOR ORGANIC INSULATING RESINS BY OPTICAL LOSS ANALYSIS, Polymer engineering and science, 35(17), 1995, pp. 1375-1380
We proposed an ''optical loss analysis'' as a novel nondestructive dia
gnosis for the thermal deterioration of insulating resins. Using an al
kyd resin film, the optical absorption loss per unit optical path leng
th and the glass transition temperature (T-g,T-DMA) by dynamic mechani
cal analysis were measured during heating tests. At longer heating tim
es, values of the optical absorption loss and the T-g,T-DMA increased
concurrently. By rescaling the heating time as a reduced time, a maste
r curve of the deterioration for the resin was obtained. Consequently,
when thermal stress is the main cause of the deterioration, one can e
stimate the degree of deterioration and theoretically the residual liv
es of resins using this optical loss analysis.