SPECTROPHOTOMETRIC DETERMINATION OF MICROGRAM AMOUNTS OF SULFUR .8. THERMO-SPECTROPHOTOMETRIC METHOD FOR TOTAL SULFUR DETERMINATION IN MINERAL-OILS

Authors
MROCZKOWSKI W CYGANSKI A
Citation
W. Mroczkowski et A. Cyganski, SPECTROPHOTOMETRIC DETERMINATION OF MICROGRAM AMOUNTS OF SULFUR .8. THERMO-SPECTROPHOTOMETRIC METHOD FOR TOTAL SULFUR DETERMINATION IN MINERAL-OILS, Chemia Analityczna, 40(4), 1995, pp. 641-647
Citations number
8
Categorie Soggetti
Chemistry Analytical
Journal title
Chemia Analityczna → ACNP
ISSN journal
00092223
Volume
40
Issue
4
Year of publication
1995
Pages
641 - 647
Database
ISI
SICI code
0009-2223(1995)40:4<641:SDOMAO>2.0.ZU;2-S
Abstract
A method for the determination of total sulfur in mineral oils has bee n developed. The method involves combustion of an oil sample in a pipe furnace in a stream of air at 1000 degrees C in the presence of CuO a nd spectrophotometric determination of the formed sulfur dioxide by pa rarosaniline method. The method can be used to determine from 2 to 50 mu g of sulfur in a 40 mg sample of oil. The linearity range of the me thod is 2-50 mu g S.