A. Onojah et al., ROUTINE DETERMINATION OF MANGANESE IN ORES BY INAA WITH AN AM-BE NEUTRON SOURCE - APPLICATION TO MANGANESE ORE-DEPOSITS IN NORTH-WESTERN NIGERIA, Journal of radioanalytical and nuclear chemistry, 201(1), 1995, pp. 25-30
A 5 Ci Am-Be isotopic neutron source was used for the routine determin
ation of manganase in ore samples. Concentration range was 0.1-35%, sa
mple mass is about 17 g, irradiation time 6 h and cooling time 2 min,
Counting was performed with a flat 3 '' x 3 '' NaI crystal for 1 h. Fo
r low concentrations, several aliquots are irradiated in identical pos
itions around the source and combined. Standards of similar compositio
n to that of the samples are made of KMnO4 mixed with Fe2O3 and SiO2.
Corrections are applied for residual differences in neutron and gamma-
absorption.