J. Crampon et al., COMPRESSIVE CREEP AND CREEP FAILURE OF 8Y(2)O(3) 3AL(2)O(3)-DOPED HOT-PRESSED SILICON-NITRIDE/, Journal of the American Ceramic Society, 80(1), 1997, pp. 85-91
The compressive creep properties of hot-pressed Si3N4-8Y(2)O(3)-3Al(2)
O(3) (wt%) have been investigated in the temperature range of 1543-160
3 K in air, The stress exponent, n, of the power creep law was determi
ned to be 1.5, and the activation energy was determined to be 650 kJ/m
ol. Transmission electron microscopy observations showed that grain-bo
undary sliding occurred with cavitation formation in the grain-boundar
y glassy phase. The quasi-steady-state creep results were consistent w
ith that of the diffusion-controlled solution-diffusion-precipitation
creep mechanism, and the distinguished failure mechanism was cavitatio
n creep damage controlled by the viscosity of the boundary glassy phas
e, The compressive creep failure time, obtained at 1573 K, in the stre
ss range of 175-300 MPa, followed the Monkman-Grant relation, indicati
ng that cavity growth was mainly controlled by the creep response of t
he material.