Y. Okamoto et al., MECHANICAL-PROPERTIES AND OXIDATION RESIS TANCE OF SILICON-NITRIDE PRODUCED FROM LOW PURITY BETA-POWDER, Nippon Seramikkusu Kyokai gakujutsu ronbunshi, 103(7), 1995, pp. 720-723
Low-cost and low-purity beta-Si3N4 powder was sintered at 1900 degrees
C for 8h in 1 MPa nitrogen gas with 2 mol% Y2O3-2 mol%A1(2)O(3) addit
ives, Fully densified bodies were obtained by the gas-pressured-sinter
ing. This material had a strength of 689 MPa and a fracture toughness
of 6.4 MPa . m(1/2), Furthermore, the high temperature strength, oxida
tion resistance, fatigue parameter were measured, The degradation of s
trength at elevated temperature was less than 5 % up to 900 degrees C,
No fatal defect was created in 100h-oxidation in 900 degrees C-air, T
he fatigue parameter was on a level with general material produced fro
m alpha-rich powder. These properties are adequate for structural mate
rial application.