Ar. Clarke et al., A NOVEL TECHNIQUE FOR DETERMINING THE 3D SPATIAL-DISTRIBUTION OF GLASS-FIBERS IN POLYMER COMPOSITES, Composites science and technology, 55(1), 1995, pp. 75-91
Over the past ten years, conventional 2D optical reflection microscopy
has become a standard tool for inferring the fibre orientation distri
butions of both short- and continuous-fibre-reinforced composites. Rec
ently, there has been a growing interest in determining the correlatio
n of 3D fibre waviness and ply misalignment with compressive strength
and failure mechanisms in unidirectional composites. Conventional opti
cal reflection microscopy could still be used to investigate these phe
nomena by the analysis of multiple, polished and prepared sample secti
ons and correlating fibre images between sections. However, we believe
that the non-destructive, optical sectioning inherent in the confocal
laser scanning microscope (CLSM) will make the CLSM a new standard re
search tool. 3D spatial distributions are reported for two totally dif
ferent composites: (i) continuous, unidirectional glass fibres in a mu
ltiple ply, T800 epoxy and (ii) short glass fibres in polyoxymethylene
which has been hydrostatically extruded.