G. Sartori et al., SOLVENT EFFECT IN THE FRAGMENT CONDENSATION SYNTHESIS OF CALIX(4)ARENES AND TEMPERATURE-DEPENDENT H-1-NMR STUDIES OF NEW DIHOMOMONOXAEALIXARENES, Tetrahedron letters, 36(45), 1995, pp. 8323-8326
Reaction of formaldehyde with 2,2'-dihydroxy-3,3'-di-tert-butyldipheny
(1) in basic media affords calix[4]arenes 2 or dihomomonooxacalix[4]a
renes 3 depending on the solvent (xylene or Cl2CHCHCl2) Temperature de
pendent H-1-NMR studies of compounds 3 are reported.