SYNTHESIS OF ,1-D-1',2'-G][1,3,6,2]DIOXATHIAPHOSPHOCIN-8-OXIDES

Citation
K. Anuradha et al., SYNTHESIS OF ,1-D-1',2'-G][1,3,6,2]DIOXATHIAPHOSPHOCIN-8-OXIDES, Indian Journal of Heterocyclic Chemistry, 5(1), 1995, pp. 15-18
Citations number
15
Categorie Soggetti
Chemistry Inorganic & Nuclear
ISSN journal
09711627
Volume
5
Issue
1
Year of publication
1995
Pages
15 - 18
Database
ISI
SICI code
0971-1627(1995)5:1<15:SO,>2.0.ZU;2-3
Abstract
Synthesis of 8-(alkoxy) dinaphtho [2, 1-d: 1', 2',-g][1, 3, 6, 2] diox athiaphosphocin-8-oxides is described. The initial reaction involved t he cyclization of bis (2-hydroxy-1-naphthyl) sulfide with phosphorus o xychloride in dry toluene to generate 8- chorodinaphtho [2, 1-d: 1', 2 '-g][1, 3,6,2] dioxathiaphosphocin-8-oxide. Esterification of the latt er with a variety of alcohols produced the title compounds. The compou nds were characterized by elemental analyses and spectral data.