T. Buyukyilmaz et al., IMPROVING ORTHODONTIC BONDING TO GOLD ALLOY, American journal of orthodontics and dentofacial orthopedics, 108(5), 1995, pp. 510-518
Flat tabs of cast gold alloy (n = 156) were subjected to either of thr
ee surface treatments: (1) roughening with diamond bur, (2) aluminum o
xide sandblasting, and (3) sandblasting plus tin electroplating. Mandi
bular incisor edgewise brackets were bonded with Concise (BIS-GMA resi
n) (Unitek, Monrovia, Calif.) or Superbond C&B (4-META metal bonding r
esin) (Sun Medical Co. Ltd., Kyoto, Japan), or with Concise after appl
ication of an intermediate resin. All-Bond 2 Primers A and B (Bisco De
ntal Products, Itasca, III.), or B alone. All specimens were stored in
water at 37 degrees C for 24 hours, and 60 were then thermocycled 100
0 times from 5 degrees C to 55 degrees C and back. The tensile bond st
rength testing was performed in a Lloyd 1000R machine (Fareham, Hants,
England). Alignment and uniform loading during testing were secured b
y engaging a hook in a circular ring soldered onto the bracket slot be
fore bonding. Similar control brackets (n = 24) were bonded with Conci
se to extracted human premolars and lower incisors according to a rout
ine procedure. Bond failure sites were classified by a modified ARI sy
stem. The results showed that sandblasting produced significantly stro
nger bonds to gold alloy than roughening with diamond bur. Superbond C
&B provided significantly stronger bonds to gold allay than Concise. T
here were generally insignificant differences in bond strengths betwee
n the water stored and the thermocycled specimens. Bond failures of Co
ncise to sandblasted plus tin-plated gold alloy invariably occurred at
the gold/adhesive interface, whereas those of Superbond C&B occurred
within the adhesive or in the adhesive/bracket interface. The bond str
engths obtained with Superbond C&B and sandblasted gold alloy surfaces
were comparable to those of the brackets bonded to conventionally etc
hed human teeth with Concise. Tin-plating improved the orthodontic bon
d strengths to sandblasted gold alloy only marginally. The bond streng
th of Concise to sandblasted gold alloy was significantly improved wit
h the intermediate application of A1l-Bond 2 primers A and B. It is co
ncluded that successful bonding to gold alloys is feasible with severa
l combinations and clinical recommendations for bonding brackets and l
ingual retainer wires to high-noble alloy surfaces are discussed.