F. Cebollada et al., ANGULAR-DEPENDENCE OF COERCIVITY IN ND-FE-B SINTERED MAGNETS - PROOF THAT COHERENT ROTATION IS NOT INVOLVED, Physical review. B, Condensed matter, 52(18), 1995, pp. 13511-13518
An experimental procedure is presented which allows the analysis of th
e angular dependence of the coercivity of polycrystalline samples H-c(
theta) in terms of the angular dependence of the switching field of th
e individual grains forming the material, H-s(theta'). The method is b
ased on the measurement of the remanence curves corresponding to three
different field configurations (in which the demagnetizing field is d
irected antiparallel, perpendicular, and almost parallel to the satura
ting field, respectively). By using this procedure we have studied the
angular dependence of the coercivity in sintered oriented magnets bas
ed on the Nd2Fe14B hard phase. According to our results the switching
field of the individual crystallites increases monotonically from appr
oximately 0.15H(A), H-A being the anisotropy field, for those whose ea
sy axis is oriented parallel to the demagnetizing field (theta' = 0 de
grees), to values close to H-A, for those whose easy axis is perpendic
ular (theta' = 90 degrees), and follows closely a 1/cos theta' law up
to theta' = 50 degrees. This shows that the magnetic anisotropy value
in the regions where the nucleation takes place during the reversal of
magnetization is not far from the bulk value, and also that coherent
rotation is not the determinant mechanism among those governing the nu
cleation process.