A 3.6 MeV proton irradiation of annealed Zr-2.5Nb has been performed t
o determine whether proton irradiation will enhance the precipitation
of Nb-rich beta-phase precipitates within the alpha-grains. A transmis
sion electron microscope examination of a foil after irradiation at 77
0 K for 18 h and at 720 K for 264.5 h to a total damage of 0.94 dpa re
vealed a fine dispersion of precipitates within the alpha-grains. Elec
tron diffraction analysis of the precipitates found they have lattice
plane spacings consistent with the Nb-rich beta-phase. This result is
in agreement with the beta-phase precipitation observed following neut
ron irradiation, and thus it supports the use of proton irradiation to
simulate neutron-irradiation effects in Zr-2.5Nb.