Tr. Mcnelley et al., PRECIPITATION AND RECRYSTALLIZATION DURING PROCESSING OF A SUPERPLASTIC AL-10MG-0.1ZR ALLOY, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 166(1-2), 1993, pp. 135-143
Microstructural evolution during thermomechanical processing (TMP) of
a superplastic Al-10Mg-0.1Zr (weight per cent) alloy was studied. The
TMP was carried out at 300-degrees-C and consisted of 12 rolling passe
s corresponding to a total strain of 2.5. Superplastic elongations at
300-degrees-C exceeded 1 000% for an optimum processing schedule invol
ving a 30 min interpass anneal (IPA) time. Precipitation of the interm
etallic beta-phase (Al8Mg5) was complete at an accumulated strain of 1
.5 and the precipitate particle size and size distribution were found
to be nearly constant for the remainder of the TMP. Particle stimulate
d nucleation (PSN) of recrystallization associated with prolonged IPA
times accounted for the grain refinement necessary to support superpla
stic deformation. A model for PSN is applied to the data.