H. Biermann et al., LOCAL VARIATIONS OF LATTICE-PARAMETER AND LONG-RANGE INTERNAL-STRESSES DURING CYCLIC DEFORMATION OF POLYCRYSTALLINE COPPER, Acta metallurgica et materialia, 41(9), 1993, pp. 2743-2753
X-ray line profiles and line positions were measured on single grains
of cyclically deformed polycrystalline copper specimens unloaded from
characteristic points of the stress-strain hysteresis loop. A high-res
olution double crystal diffractometer was used to obtain local lattice
parameter changes, from which long-range internal stresses and mean s
tresses were evaluated. In the case of samples unloaded from the load-
reversal points the asymmetry of the characteristically broadened X-ra
y line profiles indicated forward and backward internal stresses preva
iling in the dislocation cell walls and cell interiors of the dislocat
ion cell structure, respectively. The changes of the long-range intern
al stresses after unloading from different points of the stress-strain
hysteresis loop can be explained in terms of the composite model. In
addition, mean strains and stresses, varying from grain to grain, coul
d be determined from the shifts of the Bragg reflections. A detailed m
icrostructure-based discussion of the elastic stored energy, evaluated
from the analysis of the stress-strain hysteresis loop, is given.