J. Kawai et al., SURFACE SENSITIVE X-RAY-ABSORPTION FINE-STRUCTURE MEASUREMENT USING SAMPLE CURRENT-INDUCED BY TOTALLY REFLECTED X-RAYS, Proceedings of the Japan Academy. Series B Physical and biological sciences, 69(7), 1993, pp. 179-184
X-ray induced current intensity and Auger electron intensity of a GaAs
wafer are measured as a function of the angle of incidence of the x-r
ays of 2-keV photon energy using synchrotron radiation. It is found th
at the current intensity curve plotted as a function of the x-ray inci
dent angle resembles the Auger electron intensity curve, but a little
difference exists which originates from the difference of the probing
depth between the two methods. It is concluded that the Auger electron
probes 10-100 angstrom depth and the sample current probes 1-10 angst
rom depth when the incident x-rays are totally reflected. On the other
hand, x-ray induced current intensity of a Si wafer is measured as a
function of incident photon energy in and out of the total reflection
condition, and by this way, x-ray absorption fine structure (XAFS) spe
ctra are obtained. It is found that the XAFS measured using the sample
current is more surface sensitive (approximately 5 angstrom) than the
Auger electron yield (approximately 50 angstrom) when the incident x-
rays are totally reflected.