Pyrolytic carbon thin (4-100 nm) films were obtained from methane in a
hot wall reactor on optically polished inert substrates by varying th
e deposition time and temperature. They were characterized by all mode
s of TEM. They are composed in majority of lamellar pyrocarbon whose t
hickness and disorder increases with increasing temperature. Isotropic
carbon islands are also observed at the upper surface of the film.