R. Nakkalil et al., THE INFLUENCE OF SOLIDIFICATION MODE ON HEAT-AFFECTED ZONE MICROFISSURING IN A NICKEL IRON BASE SUPERALLOY, Acta metallurgica et materialia, 41(12), 1993, pp. 3381-3392
The heat affected zone (HAZ) microfissuring of thermomechanically proc
essed Incoloy 903 with a duplex grain structure, has been examined wit
h a view to understand the mechanism(s) of, and to reduce the incidenc
e of microfissuring. Extensive formation of liquid films on the HAZ gr
ain boundaries primarily due to the complete constitutional liquation
of preexisting MNP phosphides, MC carbides and partial constitutional
liquation of primary MX carbide insolubles was observed. The liquid fi
lms resulted in considerable microfissuring on the long warm worked gr
ain boundaries and extensive grain boundary liquid film migration (LFM
) on the fine recrystallized grain boundaries. The liquid films formed
on the warm worked boundaries were observed to have undergone normal
solidification accompanied with the formation of dendritic gamma and t
erminal interdendritic constituents. The exclusive occurrence of LFM o
nly on the fine grains and not on warm worked grains is attributed to
the increased driving force and velocity for LFM arising due to substa
ntial interface curvature of the fine grains. It is shown that HAZ mic
rofissuring is minimized if the liquid films on the HAZ grain boundari
es can partially equilibrate by LFM instead of by normal solidificatio
n.