Bf. Antolovich et al., FATIGUE-CRACK PROPAGATION IN SINGLE-CRYSTAL CMSX-2 AT ELEVATED-TEMPERATURE, Journal of materials engineering and performance, 2(4), 1993, pp. 489-496
The fatigue crack propagation (FCP) behavior of the nickel-base supera
lloy CMSX-2 in single-crystal form was investigated. Tests were conduc
ted for two temperatures (25 and 700-degrees-C), two orientations ([00
1][110] and [001][010]), and in two environments (laboratory air and u
ltra-high vacuum 10(-7) torr). Following FCP testing, the fracture sur
faces were examined using scanning electron microscopy (SEM). The FCP
rates were found to be relatively independent of the temperature, envi
ronment, and orientation when correlated with the conventional mode I
stress-intensity factor. Examination of the fracture surfaces revealed
two distinct types of fracture. One type was characterized by {111} f
racture surfaces, which were inclined relative to both the loading and
crack propagation directions. These features, although clearly a resu
lt of the fatigue process, resembled cleavage fractures along {111} pl
anes. Such features were observed at 25 and 700-degrees-C; they were t
he only features observed for the 25-degrees-C tests. The second type
had a macroscopically dull loading appearance, was microscopically rou
gh, and grew normal to the loading axis. These features were observed
on the specimens tested at 700-degrees-C (in both air and vacuum) and
appeared similar to conventional fatigue fractures. Although in this r
egion the crack plane was macroscopically normal to the loading direct
ion, it deviated microscopically to avoid shearing the gamma' precipit
ates. In view of the complex crack growth mechanisms, mixed fracture m
odes, and lack of any difference in FCP rates, it is hypothesized that
the correlation between FCP rates and the stress-intensity parameter
is probably coincidental. The implications for life prediction of high
er temperature turbine components based on conventional fracture mecha
nics are significant and should be investigated further.