M. Leonowicz et al., CRYSTALLOGRAPHIC AND MAGNETIC ALIGNMENT IN HOT-ROLLED PR20FE74B4CU2 ALLOYS, Journal of magnetism and magnetic materials, 166(1-2), 1997, pp. 165-171
Ingot material with the composition Pr20Fe74B4Cu2, in the form of a ci
rcular cross section billet, was hot-rolled at temperatures 800-1000 d
egrees C using a strain rate of approximately 3 s(-1). The magnetic me
asurements revealed that the crystallographic alignment, and as a cons
equence the remanence J(r) increased significantly in a direction perp
endicular to that of the rolling direction, with values of J(r) up to
1000 mT, despite the use of high strain rate processing. The anisotrop
y is considered to develop through a contribution of grain boundary li
quid phase diffusion and rotation of the initial plate-shaped primary
crystals. It is possible that this induced alignment was more pronounc
ed at high temperatures as a result, it is proposed, of a higher diffu
sion rate in the liquid grain boundary phase. In contrast, the coerciv
ity was found to decrease at higher rolling temperatures as a result o
f the coarsening of the microstructure.