In. Stankov et Vv. Lysenko, TITRIMETRIC DETERMINATION OF O-CHLOROBENZALMALONONITRILE AND SOME OTHER ALPHA,BETA-UNSATURATED COMPOUNDS, Journal of analytical chemistry, 52(2), 1997, pp. 171-177
Four titrimetric procedures for the determination of o-chlorobenzalmal
ononitrile using 2-dialkylaminoethanethiols, a methanolic solution of
sodium hydroxide, and aqueous solutions of alkali cyanides as reagents
, among them direct titration of o-chlorobenzalmalononitrile with an N
aCN solution with self-indication of the equivalence point and back ti
tration of excess NaCN by the Leibig-Deniges method, were developed.