H. Mahfuz et al., FAILURE MECHANISMS IN MISSION-CYCLED CARBON-CARBON COMPOSITES UNDER FLEXURAL LOAD AT ROOM AND ELEVATED-TEMPERATURES, Journal of Materials Science, 28(21), 1993, pp. 5880-5886
The response of quasi-isotropic laminates of SiC coated carbon/carbon
(C/C) composites under flexural load was studied. Mission-cycled as we
ll as virgin specimens were tested to compare the thermal- and pressur
e-cycling effects. Variation of flexural strength and stiffness with t
emperature was investigated to study the load-deflection behaviour and
the thermal stability of C/C composites up to 1371-degrees-C. Increas
e in flexural strength and stiffness were observed with the rise in te
mperature. A distinct shift in failure modes from compressive to tensi
le was found with the mission-cycled specimens with the increase in te
st temperatures, while the failure mode for virgin material was found
always on the tensile side. Change in the load-deflection behaviour wa
s examined and increase in non-linearity of the stress-strain behaviou
r with the mission cycling was observed. Although the number of test s
pecimens was few, Weibull characterization on the flexure data was per
formed to study the variation of Weibull modulii and the characteristi
c lives. Failed, as well as untested, specimens were C-scanned to iden
tify the location and the extent of the damaged zone. Post-failure ana
lyses through optical microscopy and scanning electron microscopy were
performed to study the damage growth and failure mechanisms, Degradat
ion and separation of the porous matrix structure, localized damage of
the reinforcing fibres in the transverse direction, complete fibre bu
ndle failure in the mission-cycled specimens, and delamination near th
e loading zone were observed.