A short-lived, delayed neutron activation technique has been investiga
ted to determine the content of cryolite (Na3AlF6) in core samples, by
the detection of fluorine through the fast neutron reaction F-19(n, a
lpha)N-16. The resultant gamma-rays in the energy range of 2.84-8.14 M
eV measured for pure cryolite and background samples, established that
cryolite concentrations > 13.6 wt% in rock samples could be estimated
with uncertainties of about +/-4.3 wt%. The results are very satisfac
tory for exploration purposes.