A SOLUBLE BENZODIFLUORANTHENE DERIVATIVE BY DEHYDRATION OF AN OXYGEN-BRIDGED PRECURSOR

Citation
H. Schirmer et al., A SOLUBLE BENZODIFLUORANTHENE DERIVATIVE BY DEHYDRATION OF AN OXYGEN-BRIDGED PRECURSOR, Chemische Berichte, 126(11), 1993, pp. 2543-2546
Citations number
17
Categorie Soggetti
Chemistry
Journal title
ISSN journal
00092940
Volume
126
Issue
11
Year of publication
1993
Pages
2543 - 2546
Database
ISI
SICI code
0009-2940(1993)126:11<2543:ASBDBD>2.0.ZU;2-3
Abstract
Synthesis and characterization of the alkyl chain-substituted benzodif luoranthene 6 are described. The final synthetic step involves an acid -promoted dehydration whose conversion is determined to be quantitativ e. The solubilities of compounds 4e, 5, and 6 are qualitatively correl ated with structural features. The molecular structure of 6 in the cry stal is elucidated by an X-ray structure analysis.