NEW APPARATUS FOR CERAMIC TEXTURING WORKING UNDER UNIAXIAL-STRESS ANDIN A MAGNETIC-FIELD

Citation
Jg. Noudem et al., NEW APPARATUS FOR CERAMIC TEXTURING WORKING UNDER UNIAXIAL-STRESS ANDIN A MAGNETIC-FIELD, Superconductor science and technology, 6(11), 1993, pp. 795-798
Citations number
14
Categorie Soggetti
Physics, Applied","Physics, Condensed Matter
ISSN journal
09532048
Volume
6
Issue
11
Year of publication
1993
Pages
795 - 798
Database
ISI
SICI code
0953-2048(1993)6:11<795:NAFCTW>2.0.ZU;2-U
Abstract
We have developed a new versatile apparatus combining the effect of ho t pressing and the effect of magnetic field to texture HTSC (high-temp erature superconductor) ceramics. The experimental set-up allows appli cation of uniaxial stress up to 1100-degrees-C under a maximum pressur e of 60 MPa, in a controlled atmosphere and a magnetic field of 8 T. W e have optimized the cycle for stress application along with the therm al cycle to produce highly-textured ceramics. In this paper, we descri be the stress and thermal cycles used to texture Bi-Pb-Sr-Ca-Cu-O (222 3 phase) ceramics. We present the physical and chemical characterizati ons of the samples which show a strong degree of crystallite orientati on.