Monolithic nanocomposite aerogels of two aluminosilicate compositions
have been prepared and characterized by different techniques. The resu
lts show that high surface area and mesoporosity can be preserved in t
he above nanocomposite aerogels by heating at 1000-degrees-C, unlike t
he single component aerogels. The presence of alumina as a second phas
e prevented their densification which resulted in surface areas on the
order of 500-600 m2/g and mesopores of about 5-6 nm in diameter after
heat treatment at 1000-degrees-C. These novel nanocomposite aerogels
are expected to find applications at high-temperatures in separations,
insulation, catalysis, etc.