N. Balagopal et al., COLLOIDAL PROCESSING OF SOL-SPRAYED CERAMIC PARTICULATE COMPOSITES, Journal of the European Ceramic Society, 12(6), 1993, pp. 449-453
Sol-gel based preparative procedures are capable of reducing the probl
ems of particle size distribution, purity and homogeneity of the phase
s in ceramic particulate composites. However, the tendency for agglome
ration of these powders creates serious problems for processing to sha
pes. The present work is a critical study of the preparation of 10% ce
ria-alumina composite particulates, by a mixed sol-spray technique fol
lowed by pressure filtration for final consolidation. The powder was a
lso compacted by ceramic uniaxial dry pressing for comparison purposes
. The details of powder preparation, powder characteristics, filtratio
n conditions, compaction and sintering behaviour and the final sintere
d microstructural features of the compacts have been studied and evalu
ated.