Jr. Treglio et al., DEPOSITION OF TIB2 AT LOW-TEMPERATURE WITH LOW RESIDUAL-STRESS BY A VACUUM-ARC PLASMA SOURCE, Surface & coatings technology, 61(1-3), 1993, pp. 315-319
Titanium diboride is a very hard, abrasion resistant material that has
been identified as having value as a potential erosion resistant mate
rial to coat turbine components. It is desired to deposit this coating
on materials that, for varying reasons, are adversely affected by the
temperatures at which standard physical vapor deposition processes op
erate. Deposition at lower temperatures in such processes yields a coa
ting with high residual compressive stress. In the present work, titan
ium diboride has been deposited on various substrate materials by cath
odic arc. A technique has been developed, using pulsed high voltage bi
as applied to the target, that reduces the compressive stress in the c
oating, even when the coating is deposited at near room temperatures.
This pulsed-bias method makes it possible to deposit TiB2 to a thickne
ss of more than 10 mum at near room temperature, making the process su
itable for deposition onto temperature sensitive materials.