The growth mechanism of the sulphide scale on amorphous Al-Mo alloys h
as been studied using a marker technique. A very thin (5 nm) gold mark
er film was deposited onto the surface of the Al-46Mo alloy and after
sulphidation for 5 hours at 1073 K the gold marker distribution in the
scale has been determined by RBS. It has been found that the main par
t of the marker remained at the scale surface indicating that the doub
le-layer sulphide scale on the discussed alloy is growing by the inwar
d diffusion of sulphur.