Pure C-60 single crystals have been obtained from benzene solution and
characterized by X ray measurements. An hexagonal structure which is
a multiple of the well established fee structure is confirmed. These c
rystals (which have a platelet form) are very brittle and sensitive to
the potassium insertion : whatever the temperature of insertion (from
100 degrees C to 200 degrees C), the single crystal was completely br
oken and a saturated K6C60 phase has been characterized.