O. Heczko et P. Ruuskanen, MAGNETIC-PROPERTIES OF COMPACTED ALLOY FE73.5CU1NB3SI13.5B9 IN AMORPHOUS AND NANOCRYSTALLINE STATE, IEEE transactions on magnetics, 29(6), 1993, pp. 2670-2672
The uniaxial cold and hot pressing and shock wave compaction were used
to produce ring cores from amorphous Fe73.5Cu1Nb3Si13.5B9 powder and
ribbon. The microstructure of the cores was checked by X-ray diffracti
on. No crystallization was found during compaction. The magnetic hyste
resis loops of the cores were measured in as-compacted state and after
various heat treatment. Coercive force H(c) and permeability mu(r) we
re determined as a function of annealing temperature between 400 and 6
50-degrees-C. Annealing to produce nanocrystalline state was found to
improve magnetic properties considerably. The lowest H(c), about 10A/m
and the highest mu(r), about 10(5) found for ribbon-compacted sample
are close to those measured in the wound ribbon. The observed magnetic
behaviour of the samples compacted in different ways is explained on
the basis of stress and creep-induced anisotropies.